ORGLIST:Re: Everybody digest, Vol 2 #146 - 1 msg

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From: Lakshmipathi (plpathi$##$hotmail.com)
Date: Mon Nov 15 2004 - 10:50:10 EST


Hi
I think you could mix methyl iodide and TPP in benzene and leave it stirring
for 6-8hrs. You could take TPP more and then after 8h, the isolated solid
should be filtered and washed with benzene to remove excess MeI. This is
what is used for undeutrated MeI and TPP reaction and only the difference is
MeI is taken in excess rather than TPP...
Lakshmipathi
Email; plpathi$##$hotmail.com

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Subject: Everybody digest, Vol 2 #146 - 1 msg

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> Dear all,
> I am badly in need of procedure to prepare methyl-d3-triphenylphosphonium
iodide from d3-methyl iodide and triphenyl phosphine.
> It will be very kind of if somebody gets me the procedure.
> Thanks in advance
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> Shambabu Joseph Maddirala
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> <DIV><FONT size=2>Dear all,</FONT></DIV>
> <DIV><FONT size=2>I am badly in need of procedure to prepare
methyl-d3-triphenylphosphonium iodide from d3-methyl iodide and triphenyl
phosphine.</FONT></DIV>
> <DIV><FONT size=2>It will be very kind of if somebody gets me the
procedure.</FONT></DIV>
> <DIV><FONT size=2>Thanks in advance</FONT></DIV></DIV><BR><BR>Shambabu
Joseph Maddirala<br>Postdoctoral Fellow <br>Department of
Chemistry,<br>National Tsing Hua University,<br>Hsinchu 30013, Taiwan,
R.O.C<br>Tel: Off: (03) 5715131-5640<p>
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