Re: ORGLIST:N-(benzoyl)-L-glutamic acid synthesis

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From: Vortigern (thomas$##$jefferson911.fsnet.co.uk)
Date: Mon Feb 09 2004 - 18:49:13 EST


I suspect that the pH of your rxn is too high, your hydrolysing the acid chloride before it has a chance to react. Try running it around pH 8 and/or use a biphasic system with say DCM.

Tom

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