ORGLIST: Lawesson's reagent in polar solvents...

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From: Gianluca.Sbardella$##$uniroma1.it
Date: Fri Dec 14 2001 - 08:29:23 EST


 

Dear colleagues,
I tried to achieve the complete thi= onation of a pentapeptide using Lawesson's reagent. Alas, this compound is = not soluble in dioxane or THF which I used for this reaction. Did anybody e= ver try a different solvent, i.e. methanol?

Thank you very much in a= dvance,

Dr. Gianluca Sbardella
Università degli studi di S= alerno
Dip. Scienze Farmaceutiche
Via Ponte Don Melillo
84084 - Fi= sciano (SA)
Italy

tel: +39089962819
fax: +39089962828
email= : gsbardella@unisa.it
gianluca.sbardella@uniroma1.it

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